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A process for separating a mixture of SF 6 and nitrogen or air, said process comprising: contacting the mixture in at least one adsorption stage with hydrophobic zeolites having an SiO 2 /Al 2 O 3 ratio of at least 80 and a pore diameter of 4 to 7 Å (0.4 to 0.7 nm) to preferentially adsorb SF 6, and recovering nitrogen or air depleted in SF 6.
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